National Metallurgical Laboratory, Jamshedpur
 

Testing Facilities

Sl.No.
Description
I
Metallography Structure
A.(i)   Examination of micro-structure 
         and macro-structure and   
          sulphur print including cutting,
          grinding and preparing the    
          specimen and  interpretation 
          of results with  photograph
(ii)     Metallography in-situ
B. Microhardness
II
Heat treatment
Heat treatment like annealing, normalising oil quenching, water quenching and tempering etc. including preparation of the specimen
Hardness Tests
Hardness tests by Vikcer/Brinell/Rockwell/ Pyramid hardness tests
III
Chemical Analysis
Conventional method
 
Instrumental methods (where standards are not readily available)
 
Instrumental methods (where standards are available)
 
Spectrographic method for
i)     Quantitative analysis
ii)   Qualitative analysis
iii)  Hydrogen content in metal sample
IV
Corrosion Tests
Atmospheric test (Marine and industrial)
Wetherometer test (humidity, condens-tion, temperature, radiation rays) for coatings
Evaluation of Inhibitor
Lubricant corrosion
Evaluation of metals & alloys in specific environment
Evaluation of Sacrificial anode
Electrochemical test (any type)
 
Tests for metallic and non-metallic
i)                    Adhesion
ii)                   Hardness
iii)                 Porosity
iv)                 Thickness
v)                  ARE salt drop test for salt spray tests
vi)                 CRL breaker test
 
 
a)      Tests for stainless steel
i)                    Copper sulphate- suphuric acid test
ii)                   Stress corrosion cracking susceptibility test
iii)                 Boiling nitric acid test
iv)                 Salt spray test
v)                  Copper strip corrosion test
vi)                 Stress corrosion test
vii)               Wheel test for inhibitor
 
V
Physical Tests
SEM Photography
SEM + EDX analysis
SEM hot stage upto 1200 Deg.C
 
Qualitative X-ray ddefraction for Normal 2 deg./m diffractogramme (without interpretation)
Identification (presence/absence of Upto 5 specified phases
Identificiation (presence/absence of  Each additional phases
 
Quantitative estimation of crystalline Phases (standard to be given by the party)
 
Particle size (crystallite size)
 
i)   Residual stress on ferrous sample : Quantitative analysis when XEC of material available
 
ii)  Residual stress on non-ferrous sample: Qquantitative analysis when XEC of material are available)
 
iii) Determination of X-ray Elastic constants
iv) Residual stress on-site in-situ components
 
 Structure determination and lattice Parameter measurement of crystalline Constituents
 
 TEM examination of sample with 2 copies of prints/negative
 
 TEM examination as above plus EDAX micro analysis
 
VI
Magnetic Material Testing
Heat treatment and d.c magnetic testing of soft magnetic materials by ballistic method (determination of maxm. Permeability, coercive force, remanence and magnetic induction)
i)    Standard treatment tests (on ring samples)
ii)      Winding charges
iii)     Testing charges
iv)    Aging charges (on ring samples at 100 deg.C/100 hrs)
v)      Retesting after aging
 
Determination of electrical resistivity (by Kelvin Bridge method)
Permanent magnet testing (Remanence, coercive force and max. Energy poduct)
 
Thermal test of materials for
i)        Temperature variation of electrical resistivity
ii)      Differential scanning calorimetry from RT to 0.80 deg.C
VII
Mechanical Tests
Impact test on Notched Bar Izod or Charpy
At room temperature including specimen preparation
At sub-zero temperature upto –50 deg.C on prepared sample
 
Extra charge for charpy sample preparation with one notch
VIII
Tensile Test
At room temperature on prepared sample (duplicate test)
At room temperature on prepared sample with proof stress determination
At high temperature upto 750 deg.C on prepared sample
At high temperature upto 750 deg.C on prepared sample with proof stress determination
Wire rope testing at room temperature Gripping device if any
Wire/rod upto and including 3/8” without machining at room temperature
Sub-zero temperature upto –50 deg.C on prepared sample
Rods above 3/8” dia without machining
IX
Compression Test
At room temperature on prepared sample (cube or cylinder)
At high temp. Upto 750 deg.C on prepared sample
Extra charge for sample preparation
Preparation of spring sample
X
Torsion Test
Bare wires upto 3mm dia at room temp.
Surface dressing if required at extra cost
At high temp. Upto 750 deg.C on bare wire of 3mm dia
XI
Transverse Test
Testing of cast iron bar including measurement of deflection on prepared sample
XII
Bend Test
Specimen ready for testing
Extra charges for preparing the test piece
Fracture toughness test.
Extra cost for sample preparation
Fatigue test .
Extra cost for sample preparation
XIII
Ductility Test (by alternate bending)
a)      Wire 1 to 3mm dia
b)      Sheet 1 to 3mm thick
c)       Swift cupping sheets upto 1-3mm thick
d)      Olsen cupping
XIV
Wear Test
a)      Prepared test piece
(Extra charge for preparation of test pieces i.e. circular disc and test pieces)
 
 
Accelerated life test of heating elements (wire 300mm in length & 0.71mm in dia)
XV
Creep Test
a)      Stress rupture test in multi-specimen creep testing machine upto 700 deg.C
b)      Creep test in single specimen creep testing machine upto 700 deg.C
XVI
Refractories Test
a)      Petrographic analysis (qualitative) (sample preparation and studies)
b)      Particle size determination including sample preparation sidegraph
 
PCE Determination
Refractories under load
Permanent dimensional changes (PLC)
Cold crushing strength including sample preparation
Modulus of rupture
a)      Thermal expansion test 0 deg. to 1500 deg. C
b)   Thermal conductivity  test 0 – 800 deg. C temp
Aparent porosity, specific gravity and bulk density
True specific gravity (Helium density)
Resistance to slag attack
High temp. Creep
HOT MOR
DTA/DTG
Pore & Pore size distribution
XVII
Iron Ores and Coal samples
a)      Reducibility test of iron bearing materials
b)      Rotary reduction test (linder plus modified linder test)
c)       Crushing strength of iron ore pellets
d)      Swelling test of iron ore pellets
e)      Determination of reduction degradation index of iron bearing material
f)        Low temp. Breakdown test on iron ore/sinter/pellets
g)      High temp. Breakdown test on iron ore/sinter/pellets
h)      Softening test on iron bearing material
i)        Thermal degradation of iron ores (oxidising atmosphere)
j)        Static bed matching reduction test of iron ores/coal
k)      Tumbler test on iron ore/pellets/sinters
l)        Shatter test on iron ore/pellets/sinters
m)    Reactivity determination of coal, coke and char
n)      Determination of porosities (macro & micro) of iron ores/sinters/pellets
o)      Oxiation of DRI
p)      Determination of ash fusion temp.
q)      Reactivity of limestone/dolomite
r)       Decripitation of lime
XVIII
Testing of Bentonite
a)      Crushing, grinding and shieving
b)    Sampling
b)      Determination of moisture 
      content
c)       Determination of gel valfue
d)      Determination of swelling index
e)      Methylene blue test
f)        Determination of liquid limit capacity
g)      Determination of total base exchange value
h)      Determination of sintering temperature range
 
i)        Tests for bonding
       characteristics *
j)        Casting characteristics **
k)      Complete tests for bentonite
l)        Bench scale tests for kbentonites and other bonding clays for their amanability for base exchange
a)       Before and after activation tests will be done (2400/2)
b)       Tests for activation
 
XIX
Testing of Moulding Sands
a)      Sampling
b)      Determination of clay content
c)       Mechanical grading
d)      Determination of sintering temp. Range
e)      Complete sand testing (Moulding characteristics)
XX
Evaluation of dextrine or other cellustic material as foundry biner
a)      Determination of melting point
b)      Determination of gas content
c)       Determination of ash content
d)      Determination of loss on ignition (LOI)
e)      Determination of water stability content
f)        Determination of hot and cold tensile strength
 
 
Endurance test (As per ISI specification)
 
Continuous electrical conductivity test
 
Thermal conductivity
 
Viscocity test
 
Cold bonding strength
I
Computer utilisation
 
Laboratory Scale Mineral Processing Projects
 
Complete laboratory (bench) scale mineral processing investigation involving studies for recovery of one mineral including petrology and chemical analysis
 
Development of flowsheet with mass balance, schematic layout, listing of equipment etc. based on bench scale studies
 
Complete laboratory scale mineral processing investigation involving studies for recovery of two or more minerals including petrology and chem. analysis
 
Development of flowsheet with mass balance, schematic layout, listing of equipment etc. based on bench scale studies (Ref.3 above)
 
Petrological studies for one major mineral
 
Chemical analysis (powder sample)
 
  
Lab. Scale tests/studies of a single mineral processing unit operation under pre-determined conditions including material preparation, reagent cost (if any) and chemical analysis of maximum 4 radicals
a)      Flotation
b)      Tabling
c)    Jigging
c)       Bond’s work Index Determination
d)      Leaf filtration
e)      Settling test
f)        Heavy media test (4 diff. Densities)
g)      Electrostatic separation
h)      Crushing strength
i)        Size analysis
i)                    Size analysis (cyclosizing)
ii)                   Size analysis (200mm to 200 mesh)
iii)                 Sample preparation only (10 mesh to 200 mesh)]
             (200 mm to 200 mesh)
iv)                 Size analysis (instrumental/sediment/laser)
j)        Magnetic separation (LIMS/WHIMS)
(at fixed intensity)
k)      Attrition scrubbing
l)        Tumbler test
m)    Shatter test
n)      Grindability test
o)      Hydrocyclone
p)      Multigravity separation
q)      Duplex concentrator
r)       BM Vanner
s)       Mineral Separator
t)        Sink-float studies at 4 different densities
u)      Bulk density/Sp. Gr.
v)      Pelletisation (10 kg max.)
w)     Viscosity Measurement
x)      Zeta Potential Measurement
y)      Porosity measurement
z)       Proximate analysis of coal
aa)   Centrifugation
bb)   Turbidity measurement
cc)    Conductivity measurement
dd)   Thin section preparation
ee)   Petrological sample mounting, polishing
PILOT PLANT SCALE INVESTIGATION
 
Complete pilot pllant scale mineral beneficiatlion investigation (quantity of ore to be specified by NML)